[Uni Tübingen] - [Mat.-Nat. Fakultät] - [Fachbereich Chemie] - [Anorg. Chemie] - [Klaus Eichele] - [Publications] - List of Publications

Publications Klaus Eichele

see at ORCiD


Contents [2017] [2016] [2015] [2014] [2013] [2012] [2011] [2010] [2009] [2008] [2007] [2006] [2005] [2004] [2003] [2002] [2001] [2000] [1999] [1997] [1996] [1995] [1994] [1993] [1992] [1991] [1990]
Clicking on the reference brings you to the abstract, clicking on the DOI to the publisher's page.

    --- 2017 --- [UP]

  1. P. Meixner, K. Batke, A. Fischer, D. Schmitz, G. Eickerling, M. Kalter, K. Ruhland, K. Eichele, J. E. Barquera-Lozada, N. P. M. Casati, F. Montisci, P. Macchi, W. Scherer:
    J(Si,H) Coupling Constants of Activated Si-H Bonds
    J. Phys. Chem. A 2017, 121(38), 7219-7235.
    DOI: 10.1021/acs.jpca.7b05830
  2. R. Schmidt, M. Strobele, K. Eichele, H.-J. Meyer:
    Crystal Structure and Luminescence Investigations of the Nitridomagnesoaluminates Mg3AlnNn+2 with n=1, 2, 3
    Eur. J. Inorg. Chem. 2017(20), 2727-2735.
    DOI: 10.1002/ejic.201700255
  3. J. Schneider, C. P. Sindlinger, K. Eichele, H. Schubert, L. Wesemann:
    Low-Valent Lead Hydride and Its Extreme Low-Field H-1 NMR Chemical Shift
    J. Am. Chem. Soc. 2017, 139(19), 6542-6545.
    DOI: 10.1021/jacs.7b01856
  4. J.-J. Maudrich, C. P. Sindlinger, F. S. W. Aicher, K. Eichele, H. Schubert, L. Wesemann:
    Reductive Elimination of Hydrogen from Bis(trimethylsilyl)methyltin Trihydride and Mesityltin Trihydride
    Chem. Eur. J. 2017, 23(9), 2192-2200.
    DOI: 10.1002/chem.201605317
  5. D. Schmid, A. Seyboldt, K. Eichele, D. Kunz:
    Synthesis of a lithium-cyclopentadienide complex by addition of LiNTf2 to a zwitterionic fulvalene
    Dalton Trans. 2017, 46(1), 29-32.
    DOI: 10.1039/c6dt03355e
  6. --- 2016 --- [UP]

  7. W. Scherer, P. Meixner, K. Batke, J. E. Barquera-Lozada, K. Ruhland, A. Fischer, G. Eickerling, K. Eichele:
    J(Si,H)-Kopplungskonstanten in nicht-klassischen Übergangsmetallsilankomplexen
    Angew. Chem. 2016, 128(38), 11846-11850.
    DOI: 10.1002/ange.201604001  
    J(Si,H) Coupling Constants in Nonclassical Transition-Metal Silane Complexes
    Angew. Chem. Int. Ed. 2016, 55(38), 11673-11677.
    DOI: 10.1002/anie.201604001
  8. J. Schneider, K. M. Krebs, S. Freitag, K. Eichele, H. Schubert, L. Wesemann:
    Intramolecular Tetrylene Lewis Adducts: Synthesis and Reactivity
    Chem. Eur. J. 2016, 22(28), 9812-9826.
    DOI: 10.1002/chem.201601224
  9. J. Arras, K. Eichele, B. Maryasin, H. Schubert, C. Ochsenfeld, L. Wesemann:
    Intermolecular (119)Sn,(31)P Through-Space Spin-Spin Coupling in a Solid Bivalent Tin Phosphido Complex
    Inorg. Chem. 2016, 55(9), 4669-4675.
    DOI: 10.1021/acs.inorgchem.6b00573
  10. --- 2015 --- [UP]

  11. M. Krieg, F. Reicherter, P. Haiss, M. Stroebele, K. Eichele, M.-J. Treanor, R. Schaub, H. F. Bettinger:
    Aufbau eines intern B3N3-dotierten Nanographenmoleküls
    Angew. Chem. 2015, 127 8402-8404.
    DOI: 10.1002/ange.201412165  
    Construction of an Internally B3N3-Doped Nanographene Molecule
    Angew. Chem. Int. Ed. 2015, 54(28), 8284-8286.
    DOI: 10.1002/anie.201412165
  12. A. Seyboldt, B. Wucher, S. Hohnstein, K. Eichele, F. Rominger, K. W. Toernroos:
    Evidence for the Formation of Anionic Zerovalent Group 10 Complexes as Highly Reactive Intermediates
    Organometallics 2015, 34(12), 2717-2725.
    DOI: 10.1021/om500836m
  13. K. M. Krebs, J. Wiederkehr, J. Schneider, K. Eichele, H. Schubert, L. Wesemann:
    η3-Allylkoordination an Zinn(II) – Reaktivität gegenüber Alkinen und Benzonitril
    Angew. Chem. 2015, 127 5593-5597.
    DOI: 10.1002/ange.201500386  
    η3-Allyl Coordination at Tin(II) – Reactivity towards Alkynes and Benzonitrile
    Angew. Chem. Int. Ed. 2015, 54, 5502-5506.
    DOI: 10.1002/anie.201500386
  14. T. Gädt, J.-A. Dimmer, S. Fleischhauer, A. Frank, C. Nickl, T. Wütz, K. Eichele, L. Wesemann:
    Oxidation of Germa- and Stanna-closo-dodecaborate
    Dalton Trans. 2015, 44, 4726-4731.
    DOI: 10.1039/c5dt00099h
  15. M. Ströbele, K. Eichele, H.-J. Meyer:
    Cluster Harvesting in the WBr6–P System
    Inorg. Chem. 2015, 54(3), 989–992.
    DOI 10.1021/ic502333u
  16. U. Aygül, H.-J. Egelhaaf, P. Nagel, M. Merz, S. Schuppler, K. Eichele, H. Peisert, T. Chassé, Thomas:
    Photodegradation of C-PCPDTBT and Si-PCPDTBT: Influence of the Bridging Atom on the Stability of a Low-Band-Gap Polymer for Solar Cell Application
    Chem. Phys. Chem. 2015, 16(2), 428-435.
    DOI 10.1002/cphc.201402494
  17. --- 2014 --- [UP]

  18. M. Göhner, F. Herrmann, K. Eichele, H. F. Bettinger, M. Ströbele, N. Kuhn:
    Die Strukturchemie der 2-Chalkogeno-1,3,4,5-tetraisopropylimidazoline
    Z. Naturforsch. B 2014, 69, 1384–1394.
    DOI 10.5560/ZNB.2014-4189
  19. H. Scheel, J. Wiederkehr, K. Eichele, H. A. Mayer, F. Winter, R. Pöttgen, L. Wesemann:
    Dinuclear copper complexes: coordination of Group 14 heteroborates
    Dalton Trans. 2014, 43(31), 11867-11876.
    DOI 10.1039/c4dt01242a
  20. J. Henning, K. Eichele, R. F. Fink, L. Wesemann:
    Structural and Spectroscopic Characterization of Tin–Tin Double Bonds in Cyclic Distannenes
    Organometallics 2014, 33(14), 3904–3918.
    DOI 10.1021/om500645b
  21. N. Dettenrieder, C. O. Hollfelder, L. N. Jende, C. Maichle-Mössmer, R. Anwander:
    Half-Sandwich Rare-Earth-Metal Alkylaluminate Complexes Bearing Peripheral Boryl Ligands
    Organometallics 2014, 33(7), 1528–1531.
    DOI 10.1021/om401163a
  22. --- 2013 --- [UP]

  23. C. Schädle, D. Schädle, K. Eichele, R. Anwander:
    Methylaluminium-stabilisierte Seltenerdmetalldihydride
    Angew. Chem. 2013, 125(50), 13480–13484.
    DOI 10.1002/ange.201306783  
    Methylaluminum-Supported Rare-Earth-Metal Dihydrides
    Angew. Chem. Int. Ed. 2013, 52(50), 13238–13242.
    DOI 10.1002/anie.201306783
  24. J. Arras, K. Eichele, L. Wesemann:
    Synthesis and Skeletal Transformations of Trinuclear Palladium and Nickel Phosphido Complexes
    Eur. J. Inorg. Chem. 2013(33), 5728–5737.
    DOI 10.1002/ejic.201300775
  25. --- 2012 --- [UP]

  26. V. Gierz, A. Seyboldt, C. Maichle-Moessmer, K. W. Toernroos, M. T. Speidel, B. Speiser, K. Eichele, D. Kunz:
    Dinuclear coinage-metal complexes of bis(NHC) ligands: structural features and dynamic behavior of a Cu-Cu Complex
    Organometallics 2012, 31(22), 7893-7901.
    DOI 10.1021/om300544g
  27. J.-A. Dimmer, M. Hornung, K. Eichele, L. Wesemann:
    Selenium adducts of germa- and stanna-closo-dodecaborate: coordination at platinum, structural studies and NMR spectroscopy
    Dalton Trans. 2012, 41(29), 8989-8996.
    DOI 10.1039/C2DT30478C
  28. S. Biswas, M. Mueller, C. Toenshoff, K. Eichele, C. Maichle-Moessmer, A. Ruff, B. Speiser, H. F. Bettinger:
    The Overcrowded Borazine Derivative of Hexabenzotriphenylene Obtained through Dehydrohalogenation
    Eur. J. Org. Chem. 2012(24), 4634-4639.
    DOI 10.1002/ejoc.201200322
  29. J. Henning, H. Schubert, K. Eichele, F. Winter, R. Poettgen, H. A. Mayer, L. Wesemann:
    Synthesis and Characterization of N-[2-P(i-Pr)2-4-methylphenyl]2- (PNP) Pincer Tin(IV) and Tin(II) Complexes
    Inorg. Chem. 2012, 51(10), 5787-5794.
    DOI 10.1021/ic300324s
  30. C. Toenshoff, M. Mueller, T. Kar, F. Latteyer, T. Chassé, K. Eichele, H. F. Bettinger:
    B3N3 Borazine Substitution in Hexa-peri-Hexabenzocoronene: Computational Analysis and Scholl Reaction of Hexaphenylborazine
    ChemPhysChem 2012, 13(5), 1173-1181.
    DOI 10.1002/cphc.201101025
  31. C. Nickl, K. Eichele, L. Wesemann:
    1,2-Distanna-closo-dodecaborate—a rare example of a 1,2-distannylene ligand in transition metal chemistry
    Dalton Trans. 2012, 41, 243-250.
    DOI 10.1039/C1DT11247C
  32. --- 2011 --- [UP]

  33. M. Stroebele, K. Eichele, H.-J. Meyer:
    Phosphorus-Centered and Phosphinidene-Capped Tungsten Chloride Clusters
    Eur. J. Inorg. Chem. 2011, 4063-4068.
    DOI 10.1002/ejic.201100122
  34. K. Eichele, A.-R. Grimmer:
    Phosphorus-31 and Vanadium-51 Solid-State Nuclear Magnetic Resonance Spectroscopy of beta-Vanadyl Phosphate — Effects of Homo- and Heteronuclear Spin-Spin, Electrostatic, and Paramagnetic Interactions
    Can. J. Chem. 2011, 89(7), 870-884.
    DOI 10.1139/v11-025
  35. A. Wagenpfeil, C. Nickl, H. Schubert, K. Eichele, M. A. Fox, L. Wesemann:
    1,2-Carbagerma-closo-dodecaborate as a Germanium Ligand in Coordination Chemistry – Synthesis, Structure and Reactivity
    Eur. J. Inorg. Chem. 2011(22), 3349–3356.
    DOI 10.1002/ejic.201100310
  36. C. Nickl, K. Eichele, D. Joosten, T. Langer, F. M. Schappacher, R. Pöttgen, U. Englert, L. Wesemann, Lars:
    1,1,1-Tris(distanna-closo-dodecaborat)stannat – ein tripodaler Zinnligand
    Angew. Chem. 2011, 123, 5886-5889.
    DOI 10.1002/ange.201100936
     
    1,1,1-Tris(distanna-closo-dodecaborate)stannate: A Tripodal Tin Ligand
    Angew. Chem. Int. Ed. 2011, 50, 5766-5769.
    DOI 10.1002/anie.201100936
  37. S. Fleischhauer, K. Eichele, I. Schellenberg, R. Pöttgen, L. Wesemann:
    Cobalt, Rhodium, Iridium, and Ruthenium Carbonyl Complexes with Stanna-closo-dodecaborate: 103Rh NMR, 119Sn Mössbauer Spectroscopy, and Solid-State 119Sn NMR
    Organometallics 2011, 30, 3200–3209.
    DOI 10.1021/om200301v
  38. H. Schubert, J.-A. Dimmer, F.-R. Küchle, K. Eichele, L. Wesemann:
    Homoleptic Coinage Metal Compounds of Group(IV)heteroborates
    Inorg. Chem. 2011, 50, 664-670.
    DOI 10.1021/ic102118n
  39. --- 2010 --- [UP]

  40. M. Zimmermann, D. Rauschmaier, K. Eichele, K. W. Törnroos, R. Anwander:
    Amido-stabilized rare-earth metal mixed methyl methylidene complexes
    Chem. Commun. 2010, 46, 5346 - 5348.
    DOI 10.1039/c003206a
  41. --- 2009 --- [UP]

  42. C. Nickl, D. Joosten, K. Eichele, C. Maichle-Mössmer, K. W. Törnroos, L. Wesemann:
    Synthese und Charakterisierung von Digerma-closo-dodecaborat, einem höheren Homologen des ikosaedrischen ortho-Carborans
    Angew. Chem. 2009, 121, 8061-8065.
    DOI 10.1002/ange.200903300
     
    Synthesis and Characterization of Digerma-closo-dodecaborate: A Higher Homologue of Icosahedral ortho-Carborane
    Angew. Chem. Int. Ed. 2009, 48, 7920-7923.
    DOI 10.1002/anie.200903300
  43. --- 2008 --- [UP]

  44. M. Kirchmann, K. Eichele, L. Wesemann:
    Synthesis and Characterization of the Platinum(IV) Hydride [PtH(SnB11H11)5]7-
    Organometallics 2008, 27, 6029-6031
    DOI 10.1021/om8006536
  45. M. Kirchmann, T. Gaedt, K. Eichele, L. Wesemann:
    Nickel coordination compounds of stanna-closo-dodecaborate
    Eur. J. Inorg. Chem. 2008, 2261-2265
    DOI 10.1002/ejic.200800142
  46. M. Kirchmann, K. Eichele, L. Wesemann:
    Homoleptic Cadmium and Mercury Compounds of Stanna-closo-dodecaborate
    Inorg. Chem. 2008, 47, 5988-5991
    DOI 10.1021/ic800357z
  47. M. Kirchmann, K. Eichele, F. M. Schappacher, R. Pöttgen, L. Wesemann:
    Oktaedrische Koordinationsverbindungen der Ni, Pd, Pt-Triade
    Angew. Chem. 2008, 120, 977-980.
    DOI 10.1002/ange.200704814
     
    Octahedral Coordination Compounds of the Ni, Pd, Pt Triad
    Angew. Chem. Int. Ed. 2008, 47, 963-966.
    DOI 10.1002/anie.200704814
  48. A. M. Winter, K. Eichele, H.-G. Mack, W. C. Kaska, H. A. Mayer:
    Prototropic rearrangements in cycloheptatrienyl PCP pincer iridium complexes.
    J. Chem. Soc., Dalton Trans. 2008, 527-532.
    DOI 10.1039/b712712j
  49. --- 2007 --- [UP]

  50. K.-P. Zeller, P. Haiss, M. Hartmann, K. Eichele:
    Unexpected Course of a Williamson Ether Synthesis.
    ARKIVOC 2007, VII, 291-300.
  51. --- 2006 --- [UP]

  52. B. A. Demko, K. Eichele, R. E. Wasylishen:
    A Combined Experimental and Quantum Chemistry Study of Selenium Chemical Shift Tensors
    J. Phys. Chem. A 2006, 110, 13537-13550.
    DOI 10.1021/jp064543s
  53. N. Kuhn, K. Eichele, M. Steimann, A. Al-Sheikh, B. Doser, C. Ochsenfeld:
    Wasserstoffbrückenbindungen mit Cyanidionen? Die Strukturen von 1,3-Diisopropyl-4,5-dimethylimidazoliumcyanid und 1-Isopropyl-3,4,5-trimethylimidazoliumcyanid.
    Z. Anorg. Allg. Chem. 2006, 632, 2268-2275.
    DOI 10.1002/zaac.200600157
  54. T. Gädt, K. Eichele, L. Wesemann:
    Bimetallic Zwitterionic Complexes with an Ambident Stanna-closo-dodecaborate Ligand: [1-{M(CO)5}-2,7,8-(m-H)3-{Fe(triphos)}-SnB11H11] (M = Cr, Mo, W)
    Organometallics 2006, 25, 3904-3911.
    DOI 10.1021/om060328m
  55. T. Gädt, K. Eichele, L. Wesemann:
    Bonding Modes of Stanna-closo-Dodecaborate: h1(Sn) to h3(BH) Rearrangement Reactions in Zwitterionic Stanna-closo-Dodecaborate Ruthenium Complexes
    J. Chem. Soc., Dalton Trans. 2006, 2706-2713.
    DOI 10.1039/b517138e
  56. R. Schmitt, B. Blaschkowski, K. Eichele, H.-J. Meyer:
    Calcium Tetraboride-Does It Exist? Synthesis and Properties of a Carbon-Doped Calcium Tetraboride That Is Isotypic with the Known Rare Earth Tetraborides
    Inorg. Chem. 2006, 45, 3067 -3073.
    DOI 10.1021/ic0518430
  57. T. Gädt, B. Grau, K. Eichele, I. Pantenburg, L. Wesemann:
    Ruthenium complexes with the stanna-closo-dodecaborate ligand: coexistence of h1(Sn) and h3(B-H) coordination
    Chem. Eur. J. 2006, 12, 1036-1045.
    DOI 10.1002/chem.200500761
  58. --- 2005 --- [UP]

  59. N. Kuhn, A. Abu-Rayyan, A. Al-Sheikh, K. Eichele, C. Maichle-Mößmer, M. Steimann, K. Sweidan:
    Zur Strukturchemie von 2-Methylenimidazolinen
    Z. Naturforsch. B 2005, 60, 294-299.
  60. A. M. Winter, K. Eichele, H.-G. Mack, W. C. Kaska, H. A. Mayer:
    C-H versus Ir-X (X = H, Cl) Reactivity in a Tropylium PCP Pincer Iridium Complex
    Organometallics 2005, 24, 1837-1844.
    DOI 10.1021/om049289+
  61. --- 2004 --- [UP]

  62. K. Eichele, C. Nachtigal, S. Jung, H. A. Mayer, E. Lindner, M. Ströbele:
    A Simple Molecule with a Complex Crystal Structure: Interplay of 31P Solid-State NMR Spectroscopy and Single-Crystal X-ray Diffraction in the Structure Determination of a Ruthenium Diphosphine Diamine Complex.
    Magn. Reson. Chem. 2004, 42, 807-813.
    DOI 10.1002/mrc.1433
  63. N. Kuhn, A. Abu-Rayyan, K. Eichele, C. Piludu, M. Steimann:
    Weak Interionic Interactions in 2-Haloimidazolium Hexahalotellurates(IV)
    Z. Anorg. Allg. Chem. 2004, 630, 495-497.
    DOI 10.1002/zaac.200300401
  64. I. Warad, K. Eichele, H. A. Mayer, E. Lindner:
    Supported organometallic complexes part 39: cationic diamine(ether–phosphine)ruthenium(II) complexes as precursors for the hydrogenation of trans-4-phenyl-3-butene-2-one
    Inorg. Chim. Acta 2004, 357, 1847-1853.
    DOI 10.1016/j.ica.2003.12.015
  65. N. Kuhn, A. Abu-Rayyan, K. Eichele, S. Schwarz, M. Steimann:
    Weak interionic interactions in 2-bromoimidazolium derivatives.
    Inorg. Chim. Acta 2004, 357, 1799-1804.
    DOI 10.1016/j.ica.2003.10.038
  66. --- 2003 --- [UP]

  67. A. M. Winter, K. Eichele, H.-G. Mack, S. Potuznik, H. A. Mayer, W. C. Kaska:
    Rhodium pincer complexes of 2,2'-bis(diphenylphosphino)diphenylamine
    J. Organomet. Chem. 2003, 682, 149-154.
    DOI 10.1016/S0022-328X(03)00776-9
  68. E. Lindner, M. Henes, W. Wielandt, K. Eichele, M. Steimann, G. A. Luinstra, H.-H. Görtz:
    Transition metal-catalyzed polymerization of 1,3,5-trioxane
    J. Organomet. Chem. 2003, 681, 12-23
    DOI 10.1016/S0022-328X(03)00527-8
  69. D. L. Bryce, K. Eichele, R. E. Wasylishen:
    An 17O NMR and Quantum Chemical Study of Monoclinic and Orthorhombic Polymorphs of Triphenylphosphine Oxide.
    Inorg. Chem. 2003, 42, 5085-5096.
    DOI 10.1021/ic020706p
  70. Z.-L. Lu, K. Eichele, I. Warad, H. A. Mayer, E. Lindner, Z.-j. Jang, V. Schurig:
    Supported Organometallic Complexes. XXXVIII. Bis(methoxyethyldimethylphosphine)ruthenium(II) Complexes as Transfer Hydrogenation Catalysts
    Z. Anorg. Allg. Chem. 2003, 629, 1308-1315.
    DOI 10.1002/zaac.200300067
  71. E. Lindner, I. Warad, K. Eichele, H. A. Mayer:
    Supported organometallic complexes Part 34: synthesis and structures of an array of diamine(ether-phosphine)ruthenium(II) complexes and their application in the catalytic hydrogenation of trans-4-phenyl-3-butene-2-one.
    Inorg. Chim. Acta 2003, 350, 49-56.
    DOI 10.1016/S0020-1693(02)01535-9
  72. E. Lindner, R. Zong, M. Ströbele, K. Eichele:
    Preparation, properties, and reactions of metal-containing heterocycles. CX. 1. Crystal structure of 1,1'-bis{[4-(1,10-phenanthroline-3-yl-ethynyl)- 2,5-dipropoxy-phenyl]ethynyl}ferrocene.
    Z. Anorg. Allg. Chem. 2003, 629, 587-588.
    DOI 10.1002/zaac.200390097
  73. E. Lindner, R. F. Zong, K. Eichele, U. Weisser, M. Ströbele:
    Preparation, properties, and reactions of metal-containing heterocycles, 109. Synthesis and structure of redox-active heterotetranuclear molecular polygons by self-assembly of two ferrocene-bridged bis(pyridines) with two transition metals
    Eur. J. Inorg. Chem. 2003, 705-712.
    DOI 10.1002/ejic.200390097
  74. Z.-L. Lu, K. Eichele, E. Lindner, H. A. Mayer:
    Supported organometallic complexes. Part 37: Synthesis and structures of diamine-bis(methoxyethyldimethylphosphine) ruthenium(II) complexes.
    Inorg. Chem. Commun. 2003, 6, 365 –369.
    DOI 10.1016/S1387-7003(02)00774-8
  75. E. Lindner, H. A. Mayer, I. Warad, K. Eichele:
    Supported organometallic complexes. Part XXXV. Synthesis, characterization, and catalytic application of a new family of diamine(diphosphine)ruthenium(II) complexes
    J. Organomet. Chem. 2003, 665, 176-185.
    DOI 10.1016/S0022-328X(02)02112-5
  76. --- 2002 --- [UP]

  77. H. A. Y. Mohammad, J. C. Grimm, K. Eichele, H.-G. Mack, B. Speiser, F. Novak, M. G. Quintanilla, W. C. Kaska, H. A. Mayer:
    C-H Oxidative Addition with a (PCP)Ir(III)-Pincer Complex
    Organometallics 2002, 21, 5775-5784.
    DOI 10.1021/om020621w
  78. E. Lindner, R. F. Zong, K. Eichele, M. Ströbele:
    Preparation, properties, and reactions of metal-containing heterocycles Part CVIII. A novel generation of rigid, nanoscaled 1,1'-ferrocenediyl-bridged bis(pyridine), bis(bipyridine), and bis(phenanthroline) ligands
    J. Organomet. Chem. 2002, 660, 78-84.
    DOI 10.1016/S0022-328X(02)01774-6
  79. E. Lindner, C. S. Ayasse, K. Eichele, M. Steimann:
    Macrocyclic Di- and Tetranuclear Osmacycloferrocenophanes.
    Organometallics 2002, 21, 4217-4225.
    DOI 10.1021/om020310l
  80. N. Kuhn, K. Eichele, M. Walker, Th. Berends, R. Minkwitz:
    Neuartige elementorganische Sauerstoffsäuren des Phosphors und Schwefels [1]
    Z. Anorg. Allg. Chem. 2002, 628, 2026-2032.
    DOI 10.1002/1521-3749(200209)628:9/10<2026::AID-ZAAC2026>3.0.CO;2-0
  81. K. Eichele, R. E. Wasylishen, J. F. Corrigan, N. J. Taylor, A. J. Carty, K. W. Feindel, G. M. Bernard:
    Phosphorus Chemical Shift Tensors of Phosphido Ligands in Ruthenium Carbonyl Compounds: 31P NMR Spectroscopy of Single-Crystal and Powder Samples and ab initio Calculations.
    J. Am. Chem. Soc. 2002, 124, 1541-1552.
    DOI 10.1021/ja0122041
  82. C. Nachtigal, S. Al-Gharabli, K. Eichele, E. Lindner, H. A. Mayer:
    Structural Studies of an Array of Mixed Diamine Phosphine Ruthenium(II) Complexes
    Organometallics 2002, 21, 105-112.
    DOI 10.1021/om0105831
  83. --- 2001 --- [UP]

  84. D. L. Bryce, G. M. Bernard, M. Gee, M. D. Lumsden, K. Eichele, R. E. Wasylishen:
    Practical Aspects of Modern Routine Solid-State Multinuclear Magnetic Resonance Spectroscopy: One-Dimensional Experiments.
    Can. J. Anal. Sci. Spectrosc. 2001, 46, 46-82.
    For a "reprint", see this page!
  85. B. Thomas, S. Paasch, S. Steuernagel, K. Eichele:
    Residual 31P, 35,37Cl Dipolar Coupling in 31P MAS Spectra of Chlorocyclophosphazenes.
    Solid State Nucl. Magn. Reson. 2001, 20, 108-117.
    DOI 10.1006/snmr.2001.0034
  86. N. Kuhn, K. Eichele, M. Walker:
    Synthesis and Structure of 1,3-Diisopropyl-4,5-dimethylimidazolium-2-sulfonate: A Carbene Adduct of Sulfur Trioxide.
    Z. Anorg. Allg. Chem. 2001, 627, 2565-2567.
    DOI 10.1002/1521-3749(200112)627:12<2565::AID-ZAAC2565>3.0.CO;2-I
  87. --- 2000 --- [UP]

  88. S. Schweizer, K. Eichele, H. P. T. Ammon, H. Safayhi:
    3-Acetoxy Group of Genuine AKBA (Acetyl-11-keto-b-boswellic Acid) is a-Configurated.
    Planta Medica 2000, 66, 781-782.
    DOI 10.1055/s-2000-9614
  89. G. M. Bernard, K. Eichele, G. Wu, C. Kirby, R. E. Wasylishen:
    Nuclear Magnetic Shielding Tensors for the Carbon, Nitrogen and Selenium Nuclei of Selenocyanates—A Combined Experimental and Theoretical Approach.
    Can. J. Chem. 2000, 78, 614-625.
  90. E. Lindner, J. Wald, K. Eichele, R. Fawzi:
    Synthesis, structure, and reactivity of ruthenium(II) complexes with a hemilabile tetradentate etherdiphosphine ligand.
    J. Organomet. Chem. 2000, 601, 220-225.
    DOI 10.1016/S0022-328X(00)00065-6
  91. M. Gee, R. E. Wasylishen, K. Eichele, J. F. Britten:
    Phosphorus Chemical Shift Tensors for Tetramethyldiphosphine Disulfide - A 31P Single-Crystal NMR, Dipolar-Chemical Shift NMR and Ab Initio Molecular Orbital Study.
    J. Phys. Chem. A 2000, 104, 4598-4605.
    DOI 10.1021/jp9944839
  92. M. Gee, R. E. Wasylishen, K. Eichele, G. Wu, T. S. Cameron, F. Mathey, F. Laporte:
    Characterization of Phosphorus Chemical Shielding Tensors in a Phosphole Tetramer: A Combined Experimental and Theoretical Study.
    Can. J. Chem. 2000, 78, 118-127.
  93. --- 1999 --- [UP]

  94. K. Eichele, G. Ossenkamp, R. E. Wasylishen, T. S. Cameron, J. F. Britten:
    Phosphorus-31 Solid-State NMR Studies of Homonuclear Spin Pairs in Molybdenum Phosphine Complexes: Single-Crystal, Dipolar-Chemical Shift, Rotational-Resonance and 2D Spin-Echo NMR Experiments
    Inorg. Chem. 1999, 38, 639-651.
    DOI 10.1021/ic9806232
  95. --- 1997 --- [UP]

  96. K. Eichele, R. E. Wasylishen, J. H. Nelson:
    Solid-State 95Mo NMR Studies of Some Prototypal Molybdenum Compounds: Sodium Molybdate Dihydrate, Hexacarbonylmolybdenum, and Pentacarbonyl Phosphine Molybdenum (0) Complexes.
    J. Phys. Chem. A 1997, 101, 5463-5468.
    DOI 10.1021/jp9712415
  97. K. Eichele, R.E. Wasylishen, K. Maitra, J.H. Nelson, J.F. Britten:
    Single-Crystal 31P NMR and X-ray Diffraction Study of a Molybdenum Phosphine Complex: (5-Methyldibenzophosphole)pentacarbonylmolybdenum(0).
    Inorg. Chem. 1997, 36, 3539-3544.
    DOI 10.1021/ic970260q
  98. K. Eichele, J.C.C. Chan, R.E. Wasylishen, J.F. Britten:
    Single-Crystal Cobalt-59 NMR Study of Tris(2,4-pentanedionato-O,O') Cobalt(III).
    J. Phys. Chem. A 1997, 101, 5423-5430.
    DOI 10.1021/jp970370i
  99. S. Kroeker, K. Eichele, R.E. Wasylishen, J.F. Britten:
    Cesium-133 NMR Study of CsCd(SCN)3: Relative Orientation of the Chemical Shift and Electric Field Gradient Tensors.
    J. Phys. Chem. B 1997, 101, 3727-3733.
    DOI 10.1021/jp970043a
  100. --- 1996 --- [UP]

  101. K.V. Ramanathan, N. Suryaprakash, C.L. Khetrapal, E.D. Becker, K. Eichele and R.E. Wasylishen:
    13C MAS NMR Spectra of cis,cis-Mucononitrile in Liquid Crystalline Media and the Solid State - Orientation of the Carbon Chemical Shift Tensors
    J. Magn. Reson. Ser. A 1996, 123, 196-200.
    DOI 10.1006/jmra.1996.0235
  102. K. Eichele, R.E. Wasylishen, R.W. Schurko, N. Burford, and W.A. Whitla:
    An Unusually Large Value of 1J(31P,31P) for a Solid Triphenyphoshine Phoshadiazonium Cationic Complex: Determination of the Sign of J from 2D Spin-Echo Experiments
    Can. J. Chem. 1996, 74, 2372-2377.
  103. N. Burford, T.S. Cameron, J.A.C. Clyburne, K. Eichele, K.N. Robertson, S. Sereda, R.E. Wasylishen and W.A. Whitla:
    Nucleophilic Addition of CH, NH, and OH Bonds to the Phosphadiazonium Cation and Interpretation of 31P Chemical Shifts at Dicoordinate Phosphorus Centers.
    Inorg. Chem. 1996, 35, 5460-5467.
    DOI 10.1021/ic960131u
  104. K. Eichele, R.E. Wasylishen, J.M. Kessler, L. Solujic and J.H. Nelson:
    Phosphorus Chemical Shift Tensors of Phosphole Derivatives Determined by 31P NMR Spectroscopy of Powder Samples.
    Inorg. Chem. 1996, 35, 3904-3912.
    DOI 10.1021/ic960095z
  105. W.L. Wilson, J. Fischer, R.E. Wasylishen, K. Eichele, V.J. Catalano, J.H. Frederick and J.H. Nelson:
    Thermal Coupling Reactions of 1-Phenyl-3,4-dimethylphosphole within the Coordination Sphere of Palladium (II).
    Inorg. Chem. 1996, 35, 1486-1496.
    DOI 10.1021/ic951307f
  106. I.V. Kourkine, M.B. Chapman, D.S. Glueck, K. Eichele, R.E. Wasylishen, G.P.A. Yap, L.M. Liable-Sands and A.L. Rheingold:
    Synthesis and Ligand Substitution Reactions of a Mesitylphosphido-Bridged Platinum(II) Dimer.
    Inorg. Chem. 1996, 35, 1478-1485.
    DOI 10.1021/ic951020i
  107. --- 1995 --- [UP]

  108. G. Wu, M.D. Lumsden, G.C. Ossenkamp, K. Eichele and R.E. Wasylishen:
    Carbonyl carbon chemical shift tensors for a typical aryl aldehyde and formaldehyde. NMR studies of the isolated 13C-2H spin pair of 3,4-dibenzyloxybenaldehyde-13Ca,2Ha.
    J. Phys. Chem. 1995, 99, 15806-15813.
    DOI 10.1021/j100043a019
  109. K. Eichele, R. E. Wasylishen, J. F. Corrigan, N. J. Taylor, A. J. Carty:
    Phosphorus-31 Chemical Shift Tensors of Phosphinidene Ligands in Ruthenium Carbonyl Cluster Compounds: A 31P Single-Crystal and CP/MAS NMR Study.
    J. Am. Chem. Soc. 1995, 117, 6961-6969.
    DOI 10.1021/ja00131a019
  110. K. Eichele, S. Kroeker, G. Wu, R. E. Wasylishen:
    Set-up Samples for 199Hg CP/MAS NMR Spectroscopy.
    Solid State Nucl. Magn. Reson. 1995, 4, 295-300.
    DOI 10.1016/0926-2040(95)00015-I
  111. K. Eichele, R. E. Wasylishen, J. S. Grossert, A. C. Olivieri:
    The Influence of Chlorine-Carbon Dipolar and Indirect Spin-Spin Interactions on High-Resolution Carbon-13 NMR Spectra of Chloroketosulfones in the Solid State.
    J. Phys. Chem. 1995, 99, 10110-10113.
    DOI 10.1021/j100025a010
  112. K. Eichele, G. Wu, R. E. Wasylishen, J. F. Britten:
    Phosphorus-31 NMR Studies of Solid Tetraethyldiphosphine Disulfide. A Reinvestigation of the 31P,31P Spin-Spin Coupling Tensor.
    J. Phys. Chem. 1995, 99, 1030-1037.
    DOI 10.1021/j100003a028
  113. --- 1994 --- [UP]

  114. G. Wu, K. Eichele, R. E. Wasylishen:
    Magic-Angle Spinning Frequency Dependent NMR Spectra Arising from a Pair of Crystallographically Equivalent Phosphorus Nuclei.
    In: "Phosphorus-31 NMR Spectral Properties in Compound Characterization and Structural Analysis"; L. D. Quin, J. G. Verkade (Eds.); VCH Publishers, 1994, pp 441-450.
  115. M. D. Lumsden, K. Eichele, R. E. Wasylishen, T. S. Cameron, J. F. Britten:
    Determination of a 199Hg-31P Indirect Spin-Spin Coupling Tensor via Single-Crystal Phosphorus NMR Spectroscopy.
    J. Am. Chem. Soc. 1994, 116, 11129-11136.
    DOI 10.1021/ja00103a030
  116. K. Eichele, R. E. Wasylishen:
    High-Resolution 113Cd CP/MAS NMR Studies of Cadmium Thiocyanate Coordination Compounds. Direct Observation of 113Cd,14N Spin-Spin Coupling Constants in the Solid State.
    Inorg. Chem. 1994, 33, 2766-2773.
    DOI 10.1021/ic00091a017
  117. K. Eichele, R. E. Wasylishen:
    A 31P NMR Study of Powder and Single-Crystal Samples of Ammonium Dihydrogen Phosphate: The Effect of Homonuclear Dipolar Coupling.
    J. Phys. Chem. 1994, 98, 3108-3113.
    DOI 10.1021/j100063a012
  118. M. D. Lumsden, R. E. Wasylishen, K. Eichele, M. Schindler, G. H. Penner, W. P. Power, R. D. Curtis:
    The Carbonyl Carbon and Nitrogen Chemical Shift Tensors of the Amide Fragment of Acetanilide and N-Methylacetanilide.
    J. Am. Chem. Soc. 1994, 116, 1403-1413.
    DOI 10.1021/ja00083a028
     
     
    Looking for information on acetanilide? Check out my "NMR of acetanilide" page!

     
  119. R. E. Wasylishen, K. C. Wright, K. Eichele, T. S. Cameron:
    Characterization of the J(115In,31P) Tensor for a 1:1 Adduct of Indium Tribromide and a Triarylphosphine.
    Inorg. Chem. 1994, 33, 407-408.
    DOI 10.1021/ic00081a003
  120. K. Eichele, R. E. Wasylishen:
    The Dipolar Splitting Ratio Method - A Convenient Approach to the Analysis of Dipolar-Chemical Shift NMR Spectra of Static Powder Samples.
    J. Magn. Reson. A 1994, 106, 46-56.
    DOI 10.1006/jmra.1994.1005
  121. --- 1993 --- [UP]

  122. K. L. Moran, T. E. Grier, W. T. A. Harrison, G. D. Stucky, H. Eckert, K. Eichele, R. E. Wasylishen:
    Synthesis and Characterization of Mixed ZnSe/GaP Semiconductor Species Included in the Sodalite Structure.
    J. Am. Chem. Soc. 1993, 115, 10553-10558.
    DOI 10.1021/ja00076a013
  123. K. Eichele, M. D. Lumsden, R. E. Wasylishen:
    Nitrogen-14 Coupled Dipolar-Chemical Shift 13C NMR Spectra of the Amide Fragment of Peptides in the Solid State.
    J. Phys. Chem. 1993, 97, 8909-8916.
    DOI 10.1021/j100137a014
    Errata: unfortunately, there is a sign error in eq. (10), the last term should have a positive sign!
  124. K. Eichele, R. E. Wasylishen, J. F. Corrigan, S. Doherty, Y. Sun, A. J. Carty:
    Observations of 1J(P,Ru) in 31P CP/MAS NMR Spectra of Solid Ruthenium Compounds.
    Inorg. Chem. 1993, 32, 121-123.
    DOI 10.1021/ic00054a001
  125. K. Eichele, G. Wu, R. E. Wasylishen:
    Unusual "AB" Spectra in High-Resolution Magic-Angle Spinning NMR Studies of Solids.
    J. Magn. Reson. 1993, A101, 157-161.
    DOI 10.1006/jmra.1993.1025
  126. K. Eichele, R. E. Wasylishen:
    Experimental Characterization of 31P Chemical Shift Tensors in Phosphine Derivatives.
    In: "Nuclear Magnetic Shieldings and Molecular Structure"; J. A. Tossell (Ed.); NATO ASI Series Vol. 386C, p 563, Kluwer Academic Publishers, Dordrecht 1993.
  127. R. E. Wasylishen, R. D. Curtis, K. Eichele, M. D. Lumsden, G. H. Penner, W. P. Power, G. Wu:
    Applications of Dipolar NMR Spectroscopy in Characterizing Nitrogen and Phosphorus Shielding Tensors.
    In: "Nuclear Magnetic Shieldings and Molecular Structure"; J. A. Tossell (Ed.); NATO ASI Series Vol. 386C, pp 297-314, Kluwer Academic Publishers, Dordrecht 1993.
  128. --- 1992 --- [UP]

  129. K. Eichele, R. E. Wasylishen:
    Indirect 113Cd,14N Spin-Spin Coupling Constants as a Structural Probe of Solid Cadmium Thiocyanate Complexes.
    Angew. Chem. 1992, 104, 1263-1265;
    DOI 10.1002/ange.19921040935
    Angew. Chem., Int. Ed. Engl. 1992, 31, 1222-1224.
    DOI 10.1002/anie.199212221
  130. K. Eichele, R. E. Wasylishen:
    Observation of nitrogen-14, carbon-13 indirect spin-spin coupling in high-resolution 13C CP/MAS spectra of solids.
    Solid State Nucl. Magn. Reson. 1992, 1, 159-163.
    DOI 10.1016/0926-2040(92)90016-3
  131. E. Lindner, R. Fawzi, H. A. Mayer, K. Eichele, W. Hiller:
    Effect of Ring Size on NMR Parameters: Cyclic Bisphosphine Complexes of Molybdenum, Tungsten, and Platinum. Bond Angle Dependence of Metal Shieldings, Metal-Phosphorus Coupling Constants, and the 31P Chemical Shift Anisotropy in the Solid State.
    Organometallics 1992, 11, 1033-1043.
    DOI 10.1021/om00039a007
  132. --- 1991 --- [UP]

  133. K. Eichele:
    Beziehungen zwischen Struktur- und NMR-Parametern von Phosphor- Verbindungen in Loesung und im Festkoerper.
    Ph. D. Thesis, University of Tuebingen 1991.
  134. E. Lindner, R. Fawzi, H. A. Mayer, K. Eichele, K. Pohmer:
    Phosphorus-31 Solid-State NMR Studies of Cyclic and Acyclic Phosphine-Metal Complexes. Determination of Chemical Shift Anisotropy, Scalar Coupling 1J(M-P) (M = 55Mn, 95/97Mo, 183W), and 55Mn Quadrupolar Coupling Constants.
    Inorg. Chem. 1991, 30, 1102-1107.
    DOI 10.1021/ic00005a041
  135. --- 1990 --- [UP]

  136. E. Lindner, M. Pabel, K. Eichele:
    Synthese alkylenverbrueckter Metallkomplexe nach der kationischen Alkylierung mit Alkandiylbis(trifluormethansulfonaten).
    J. Organomet. Chem. 1990, 386, 187-194.
    DOI 10.1016/0022-328X(90)85243-R
  137. E. Lindner, R. Fawzi, H. A. Mayer, K. Eichele, K. Pohmer:
    Darstellung und Eigenschaften von und Reaktionen mit metallhaltigen Heterocyclen. LXX. Untersuchungen ueber den Zusammenhang zwischen Konformation und chemischer Verschiebung in Phosphametallacycloalkanen.
    J. Organomet. Chem. 1990, 386, 63-77.
    DOI 10.1016/0022-328X(90)80257-Z

[ Anorg. Chemie ] | [ Go Home ] | webm@ster | last modified: 24.10.2017